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第1篇 质谱分析的研究与应用3

1-1 Reaction Mass Spectrometry3

1-2 Stereochemical Effects in Mass Spectrometry 2-Chemical Ionization Mass Spectra of Some Cyclic Glycols and Mono-and Di-saccharides Using Trimethyl Borate as Reagent Gas19

1-3 Stereochemical Effects in Mass Spectrometry 3 Detection of Chirality by Che-mical Ionization Mass Spectrometry27

1-4 Stereochemical Studies on Steroids by Mass Spectrometry(Ⅳ)：-Application of Me3SiNEt2 as a Reagent33

1-5 Stereochemical Effects in Mass Spectra-Studies on Mass Spectra of Epimers of Podophyllotoxin and Its Derivatives36

1-6 Stereochemical Effects in Mass Spectrometry43

1-7 Mass Spectrometry of Natural Products Stereochemical Studies by Reaction Mass Spectrometry49

1-8 CI Mass Spectra of Substituted Phenols with Acetone as Reagent52

1-9 Stereochemical Effects in Mass Spectrometry：Part 8—Chemical Ionization Mass Spectra of Cyclic Glycols and Monosaccharides Using Formaldehyde Dimethyl Acetal as Reagent Gas54

1-10 Stereochemical Effects in Mass Spectrometry Part 10 Reaction Mass Spectrometry of Cyclic Glycols and Monosaccharides with Methylene Chloride as Reagent Gas61

1-11 反应质谱法——超微量立体化学分析新技术67

1-12 天然有机化合物77

1-13 Stereochemical Effects in Mass Spectrometry ⅩⅢ Determination of Absolute Configuration by Fast Atom Bombardment Mass Spectrometry82

1-14 Stereochemical Effects in Mass Spectrometry ⅩⅤ Chemical Ionization of Some Substituted Alkenes Using Dichlorocarbene as the Reagent Gas90

1-15 Association of the Acylium Ion of Acids with Alcohols as an Esterification Mechanism in Chemical Ionization95

1-16 Stereochemical Effects in Mass Spectrometry-Determination of the Optical Purity of Enantiomers by Mass Spectrometry97

1-17 快原子轰击和碰撞活化质谱法研究三萜皂苷结构102

1-18 Fast Atom Bombardment and Collisional Activation Mass Spectrometry in the Structural Analysis of Steroidal Oligoglycosides106

1-19 Studies on the mass spectrometry of natural products115

1-20 天然有机化合物质谱研究121

1-21 寡糖快原子轰击质谱中碱金属加合离子应用技术的研究130

1-22 Mass Spectrometry of Oligosaccharides(Ⅰ)-Formation of theM+NH4］+ Ion of Oligosaccharides in Fast Atom Bombardment Mass spectrometry133

第2篇 天然产物化学139

2-1 当归化学成分分析研究——毛细管气相色谱-质谱法鉴定当归根挥发油成分139

2-2 Analysis of Chemical Ingredients of Angelica Sinensis——Analysis of Non-Volatile Constituents of Roots144

2-3 细花雪胆中的新成分——新葫芦素152

2-4 Determination of Volatile Constituents of Chinese Medicinal Herbs by Direct Vaporization Capillary Gas Chromatography/Mass Spectrometry156

2-5 Diterpenoid Alkaloids of Aconitum Sungpanense167

2-6 Diterpenoids From Rabdosia Henryi173

2-7 Ganschisandrine，A Lignan from Schisandra Sphenanthera178

2-8 Diterpenoids from RabdosiaJaponica Var.Glaucocalyx181

2-9 Diterpenoid Alkaloids from Delphinium Winklerianum185

2-10 A Diterpenoid Alkaloid from Aconitum Vilmorinianum Var.Patentipilum191

2-11 Bioactive Sesquiterpene Polyol Esters from Euonymus Bungeanus195

2-12 Diterpenoids from Rabdosia Pseudo-Irrorata202

2-13 Diterpenoid Alkaloids from Aconitum Vilmorrianum208

2-14 Sesquiterpene Polyol Esters from Celastrus Paniculatus213

2-15 Dihydroagarofuran Sesquiterpenoids from Celastrus Panicula Tus218

2-16 Diterpenoids from Rabdosia ParVifolia224

2-17 Diterpenoid Alkaloids from Delphinium caeruleum229

2-18 Triterpenoid Saponins from Anemone Hupehensis234

2-19 Diterpenoid Alkaloids from Aconitum Talassicum240

2-20 Oligostilbenes from Vitis Heyneana247

2-21 Diterpenoid Alkaloids from Delphinium Caeruleum252

2-22 Triterpenoid Saponins from Anemone Hupehensis256

2-23 Diterpenoids from Isodon Gesneroides261

2-24 TwoNewSesquiterpenes from CelastrusAngulatus268

2-25 Souline C and Souline D，New Diterpenoid Alkaloids From Delphinium Souliei272

2-26 A Simplified and Practical Method for Methylation Analysis of Polysaccharides275

2-27 红芪多糖RHG的分离纯化及化学结构278

2-28 Diterpenoids from Isodon Leucophyllus282

2-29 Diterpenoids from Isodon Eriocalyx288

2-30 Phenylpropanoid Glycosides from LamiophlomisRotata294

2-31 滇姜花抗肿瘤活性二萜及其光敏氧化反应的研究299

2-32 ent-Kaurene diterpenoids from Isodon Rubescens303

2-33 Two Glycosides from the Stem Bark of Tetracentron sinense309

2-34 Two New Diterpenoids from Isodon Rubescens314

2-35 卵叶银莲花全草中的新三萜皂苷316

第3篇 有机分析325

3-1 Microidentification of Aldehydes andAnines325

3-2 Two New Solvents for the Rast Method of Microdetermination of Molecular Weights332

3-3 原子吸收光度法测定还原糖和脂肪仲胺334

3-4 Study on Spin Labeling Analysis Synthesis and ESR Determination of Spin-Labeled Anti-Tumour Podophyllotoxin Derivatives337

3-5 Two-dimensional NMR Study of Ganwuweizic Acid340

3-6 Separation of Polycyclic Aromatic Hydrocarbons by Micellar E1ectrokinetic Chromatography with Aqueous Short-Chain Alcohol Solvent346

3-7 Chiral Gas Chromatographic Assay with Flame Ionization Detection for Amphetamine Enantiomers in Microsomal Incubates353

3-8 Carboxymethyl-β-Cyclodextrin for Chiral Separation of Basic Drugs by Capillary Electrophoresis359

第4篇 有机化学369

4-1 苯甲酰异硫氰用作鉴定醇类的试剂369

4-2 磺胺苯并噻唑Ⅳ.具有羧基的磺胺苯并噻唑371

4-3 甲基硅烷的气相氯化377

4-4 Acylthiosemicarbazides and Related Compounds382

4-5 The Total Synthesis of Taxamairin B386

4-6 The First Total Synthesis of(±)-Demethyl Salvicanol392

4-7 A Facial One-step Approach to Stereospecific Spirocyclic Diols from α-Hydroxy-epoxides400

4-8 新的烯丙型环氧醇重排还原反应研究403

4-9 An Efficient Synthesis of N-Trifluoroacetyl Adriamycin-14-Valerate(AD-32)407

4-10 Synthesis of Heterocyclic Compounds from 2-Phenyl-1，2，3-Triazole-4-Formy-lhydrazine410

第5篇 药物化学419

5-1 Spin-Labeled Antitumor Derivatives of Podophy llotoxin419

5-2 Anticancer Drugs Ⅱ.Synthesis and Biological Evaluation of Spin Labeled Deriv-atives of Podophyllotoxin429

5-3 Anticancer Drugs Part Ⅲ：New Spin Labelled Derivatives of Podophyllotoxin435

5-4 Synthesis and Antitumor Activity of Spin-Labeled Derivatives of Podophyllotoxin439

5-5 Studies on Spin-Labelled Peptide Nucleic Acid445

5-6 杂环化合物取代的5-氟尿嘧啶衍生物的合成及抗肿瘤活性450

5-7 A Facile and Efficient Synthesis of 4β-Aminopodophyllotoxins453

5-8 Synthesis of Novel 4β-(1，2，3-Triazol-1-y1)Podophyllotoxins as Potential Anti-tumor Drugs457

5-9 Synthesis of Spin Labeled Carbocyclic Lignan Analogue Related to Podophyllo-toxin461

5-10 The Synthesis of 6-Alkyl-5-Fluorouracil Derivatives465

5-11 A Facile and Highly Stereoselective Reductive Debromination of Anhydro-6-(R)-Hydroxyethyl-6-Bromopenicillin468

5-12 Synthesis of Novel Spin Labeled Analogues of N-(Trifluoroacetyl)-Daunorubicin470

5-13 Synthesis of 1-Arylated Derivatives of 5-Fluorouracil As Potential Antitumor Drug474

5-14 4β-氨基-4-脱氧鬼臼毒素和4β-氨基-4-脱氧-4′-去甲基鬼臼毒素的两种新合成方法477